正交试验优化乌药梯度渗漉提取工艺
Optimization of percolation extraction process of Radix Linderae gradient orthogonal test
摘 要:目的
筛选乌药梯度渗漉提取的最佳工艺条件.方法
采用正交试验设计,以乌药醚内酯的含量为指标,选用L9(33)正交表进行试验.考察乙醇浓度、乙醇用量、润药时间对乌药醚内酯含量的影响.结果
确定最佳方案为:润药时间为30min,加6倍量90%的乙醇.结论 采用梯度渗漉提取工艺是一种较好的提取乌药中乌药醚内酯的方法.
Abstract:
objective to
select the optimum
process conditions of
Lindera aggregata
gradient
infiltration
percolation
extraction. Methods orthogonal
design, with the content of linderane as index, used L9 (33)
orthogonal
test. The effect of alcohol
concentration,
alcohol consumption,
drug moistening time
on the content of
linderane. Results: to determine the optimal scheme for drug moistening time is 30min, adding 6 times amount of 90% alcohol. Conclusion the gradient percolation extraction process is a method of extraction of Radix Linderae better of linderane.
关键词:乌药;梯度渗漉;提取工艺;正交试验;乌药醚内酯;HPLC
Keywords:
Lindera; gradient
percolation; extraction process; orthogonal test; linderane; HPLC
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